Glass Reactors, Glass Reactor Manufacturer

Glass Reactors

我们的高硼硅酸盐玻璃反应釜，为您带来精准高效的卓越品质。采用德国进口搅拌电机，我们的反应釜性能可靠，历经38年仍能保持稳定运行。产品容量从1升到80升不等，符合CE、UL和ETL标准。

Key Features

High-Quality Materials: Durable high borosilicate glass.
Customization: Standard, explosion-proof, and custom models.
Safety Certified: CE certified; models meet UL/ETL standards.
Reliable Performance: German-imported stirring motors and patented corrosion-resistant bearings.
Versatile Options: Non-jacketed, single jacketed, and double jacketed designs.Available in volumes from 1 liter to 80 liters.

我们的玻璃反应器性能卓越、经久耐用，是化学合成、药物研发和实验室应用的理想之选。
我们提供可定制的玻璃反应器，助您提升实验室能力。立即联系我们！

Our Advantages in Glass Reactors

35+ Years Experience

We’ve utilized advanced machinery and R&D to provide market-leading glass reactors and equipment, ensuring top-notch performance and reliability.

130+ Patents

Our collaboration with university labs has resulted in the development of numerous innovative products, establishing us as pioneers in the field of glass reactors.

Prompt Support and Maintenance

Our dedicated team provides timely support and maintenance services, ensuring your glass reactors operate smoothly and efficiently.

Competitive Pricing

We offer our glass reactors at competitive prices, ensuring you receive excellent value without compromising on quality.

After-Sales Service

Our after-sales service ensures any issues with your glass reactor are promptly resolved, providing peace of mind and reliable operation.

Proven Safety

From over-temperature alarms to overload protection, our glass reactors ensure safe lab and industrial use.

GWSI Glass Reactors

20L Glass Reactor

GWSI 20L Glass Reactor uses high-temperature resistant borosilicate glass.

Suitable for Rare Earth Industry.

Function: Synthesizing and more

Main Data

Model: GR-20CE
Vessel Capacity: 20L
Jacket Capacity: 9L
Stirring Speed: 20-500rpm

50L Glass Reactor

GWSI 50L Glass Reactor feature in SUS 304 supporting framework with lockable casters.

Suitable for Semiconductor Industry.

Function: Synthesizing and more

Main Data

Model: GR-50CE
Vessel Capacity: 50L
Jacket Capacity: 13L
Stirring Speed: 20-500rpm

80L Glass Reactor

GWSI 80L 玻璃反应器的排放阀易于排空，无死体积。

适用于化肥行业。

功能：合成及更多

Main Data

型号：GR-80CE
容量：80升
容积容量：25升
搅拌速度：20-500转/分钟

2L Glass Reactor

GWSI 2L Glass Reactor fits for laboratory-scale material synthesis reactions.

Suitable for laboratories in universities.

Function: Mixing and more

Main Data

Model: GR-2CE
Vessel Capacity: 2L
Jacket Capacity: 1.7L
Stirring Speed: 40-500rpm

5L Glass Reactor

GWSI 5L Glass Reactor uses a patented PTFE stirrer bearing for reliable, quiet operation.

Suitable for research laboratories.

Function: Synthesizing and more

Main Data

Model: GR-5CE
Vessel Capacity: 5L
Jacket Capacity: 3L
Stirring Speed: 20-500rpm

10L Glass Reactor

GWSI equip 10L Glass Reactor with Brushless DC motor for tough stirring work.

Suitable for petrochemical engineering.

Function: Reaction and more

Main Data

Model: GR-10CE
Vessel Capacity: 10L
Jacket Capacity: 8L
Stirring Speed: 20-500rpm

Lifting Glass Reactor

GRL-10 Glass Reactor

GWSI GRL-10 Glass Reactor can rotate 120° to let you add solvent materials.

Main Data

Model: GRL-10
Vessel Capacity: 10L
Jacket Capacity: 8L
Stirring Speed: 20-500rpm

GRL-20 Glass Reactor

GRL-20 Glass Reactor has superior sealing effect .

Main Data

Model: GRL-20
Vessel Capacity: 20L
Jacket Capacity: 9L
Stirring Speed: 20-500rpm

GRL-50 Glass Reactor

GRL-50 Glass Reactor feature in lift available glass body.

Main Data

型号：GRL-50
容器容量：50升
外套容量：13升
搅拌速度：20-500转/分钟

Explosion Proof Glass Reactor

GR-5Ex Explosion Proof Glass Reactor

GWSI GR-5Ex Glass Reactor is a explosion proof glass reactor designed for lab.

Main Data

型号：GR-5Ex
容器容量：5升
外套容量：3升
搅拌速度：50-500转/分钟

GR-10Ex Explosion Proof Glass Reactor

GR-10Ex Glass Reactor is easy to add material with suitable discharge valve.

Main Data

型号：GR-10Ex
容器容量：10升
外套容量：8升
搅拌速度：50-500转/分钟

GR-50Ex Explosion Proof Glass Reactor

GR-50Ex Glass Reactor equipped with anti-explosion motor for safety.

Main Data

Model: GR-50Ex
Vessel Capacity: 50L
Jacket Capacity: 13L
Stirring Speed: 50-500rpm

Our streamlined process ensures a seamless experience from start to finish. Customers begin by inquiring and consulting with us. We then provide a standard or customized design tailored to their needs. After receiving a detailed quotation, customers confirm their order, allowing us to proceed with production. Finally, we ensure timely delivery of the high-quality glass reactors and equipment.

Customer Collaboration Process

01 Request Quote

02 Customization

03 Quotation

04 Confirmation

05 Production

06 Delivery

GWSI Manufacturing Capacity To Support Your Need

Through years of dedicated development and innovation, we have achieved remarkable success and established ourselves as leaders in manufacturing excellence. Our extensive manufacturing capabilities ensure that we can meet the diverse needs of various industries, from pharmaceuticals to petrochemicals, and academic research.

15500

Square Meters

我们生产小型实验室反应器和大型工业玻璃反应器，是中国重要的玻璃反应器供应商。

7

Workshops

专注于设计、组装、质量控制和定制，确保精准高效。

10+

Product Series

Includes single layer glass reactors, triple layer glass reactors, batch glass reactors, lifting glass reactors, and filter glass reactors.

100+

可选型号

从小型实验室玻璃反应器到大型夹套玻璃反应器，多种选择。

Glass Reactor Production Details

Glass Reactor Workshop

Large and modern facilities dedicated to the production of high-quality glass reactors.

Glass Reactor Materials

We use the highest grade raw materials to ensure durability and performance.

Glass Reactor Structure

Our glass reactors feature a strong and stable structure, ensuring reliable operation.

Glass Reactor Quality Check

Strict quality control ensures the highest standards for all glass reactors.

Glass Reactor Package

Our glass reactors are securely packaged with thickened foam to ensure safe delivery.

Glass Reactor Components

We offer a variety of long-term accessories for our glass reactors.

GWSI

Our Quality Commitment

GWSI拥有18年的ISO9001和CE认证，始终坚持国际质量管理标准。我们对品质的承诺确保了所有玻璃反应器的卓越性能。通过定期维护生产流程的卫生，我们保证所有原材料和组件都经过严格的安全测试。

GWSI代表着一流品质，确保我们的玻璃反应釜及其他设备可靠安全，适用于所有工业和实验室应用。无论您是采购玻璃化学反应釜还是定制异形玻璃反应釜，我们的认证都能为您提供卓越品质和符合全球标准的保证。选择GWSI，意味着选择经认证的品质，让您安心无忧地满足所有反应釜玻璃需求。

How GWSI Crafts Glass Reactor Vessels with Excellence

GWSI glass reactors are designed for various applications. For lab synthesis, they enhance efficiency and safety. In petrochemicals, our durable reactors meet performance needs with over 34 years of experience. For CBD decarboxylation, we offer customized solutions. In pharmaceuticals, our high-quality reactors provide one-stop support.

Glass Reactor For Lab Synthesis Reaction

GWSI laboratory glass reactors are essential in laboratory settings, enhancing efficiency and safety during synthesis reactions. Commonly used in universities and research institutions, they offer precision and reliability necessary for accurate experimental results.

Common Types

– Single Layer Glass Reactors

– Stirred Reactors

Matching Instruments:

Rotary Evaporators, Recirculating Chillers, Diaphragm Vacuum Pump, Water Circulating Vacuum Pump, Magnetic Stirrer, Thermostatic Water Bath, Condenser, etc.

Advantages of our glass reactors

Precision and Reliability: Ensures accurate experimental results.
Customization: Tailored designs to meet specific research needs, including size, material, and functionality.
Support and Maintenance: Timely technical support to ensure continuous research activities.

Glass Reactors For Petrochemical

In the petrochemical sector, GWSI jacketed glass reactors are known for their durability and ability to meet rigorous performance demands. With over 34 years of experience, our reactors support complex chemical processes efficiently.

Common Types

– Jacketed Glass Reactors

– High Pressure Glass Reactors

– Continuous Reactors

Matching Instruments:

Rotary Evaporators, Water Circulating Vacuum Pump, High Pressure Pump, Cooling System, Pressure Sensor, Online Analyzer, Automation Control System, etc.

Advantages of our glass reactors

Durability: Robust design to withstand harsh chemical processes.
Performance Efficiency: Supports high-demand chemical reactions with reliability.
Long-term Support: Over 34 years of experience backing our products.

Glass Reactor For CBD Decarboxylation

GWSI is your trusted partner for CBD processing with customized glass reactors. Efficiently complete your decarboxylation process with GWSI’s solutions.

Common Types

– Jacketed Glass Reactors

– Triple Layer Glass Reactors

– Batch Glass Reactors

Matching Instruments:

Recirculating Chillers, Vacuum Oven, Heating Mantle, Stirrer, Distillation Apparatus, Extraction Equipment, etc.

Advantages of our glass reactors

Efficiency: Customized solutions for optimal decarboxylation processes.
Consistency: Ensures uniform production quality.
Innovation: Advanced designs to support the growing CBD industry.

Glass Reactors For Pharmaceutical

GWSI supports pharmaceutical manufacturing and other industries with high-quality glass reactors. As a premier glass reactor manufacturer, we provide one-stop solutions for all your needs.

Common Types

– Jacketed Glass Reactors

– Filter Glass Reactors

– Stirred Bioreactors

– Custom Shaped Glass Reactors

Matching Instruments:

Rotary Evaporators, Diaphragm Vacuum Pump, Filter, Freeze Dryer, Laminar Flow Hood, Reaction Monitoring System, Purification System, etc.

Advantages of our glass reactors

Compliance: Meets industry standards and certifications (e.g., GMP, CE)
High Efficiency: Capable of supporting large-scale production needs.
Durability and Maintenance: Long-lasting equipment with easy maintenance to minimize downtime.

Your Premium Glass Reactors Manufacturer

GWSI is your reliable glass reactor manufacturer in China and GWSI is the designated glass reactor manufactuer and supplier for Chinese Vaccine companies. GWSI has a world-class research and development center equipped with advanced facilities where professional designers, product developers, and product support engineers work.

You can let GWSI customize glass reactor for your client requirement. Many Asian, European and South America pharmaceutical companies use GWSI customized glass reactor to develop Covid-19 vaccine products.

Glass Reactor Processing Machine

GWSI has strict glass reactor manufacturing standard. Every processing step is recorded to avoid potential quality defects.

There are complete glass reactor production line with experience workers in GWSI factory. You will get qualified glass reactor and glass reactor parts from GWSI.

Glass Reactors Quality Control

GWSI glass reactor meet CE certification requirement and many international standards. All raw materials of GWSI glass reactors come from top rated manufacturers.

GWSI make completely quality inspection for glass reactor before shipment such as running test, gas pressure and more. GWSI make glass kettle body thickness detection, there are few glass reactor manufacturers that measure the thickness of the kettle body.

Support Resource About Glass Reactors

Glass Reactors Parts List

This is the glass reactor parts list from this article.

Glass Reactors Operating Guide

You can learn how to operate the glass reactor in shortest time.

Glass Reactors Trouble Shooting

Here list the most common glass reactor trouble shooting methods.

Top50 Glass Reactor Manufacturers

This is the post of Top 50 glass reactor manufacturers.

Glass Reactors Installation Guide

This article will help you install glass reactors.

Glass Reactors Maintain Guide

You can learn to maintain glass reactor with this guide.

GWSI Glass Reactors Related Products

Refrigerated Heating Circulator

Diaphragm Vacuum Pump

Water Circulating Vacuum Pump

Glass Reactors Complete Guide

What is Glass Reactor Feature?

电子无级调速，电机无火花，安全可靠。
所有玻璃部件均采用耐高温硼硅酸盐玻璃材料制成，具有良好的物理和化学性能。
由于配备了放电开关，溶剂回收速度非常快。
整机采用不锈钢、铝合金和新型合成材料，具有防腐蚀、防锈、耐各种溶剂等优点。
标准化的连接方式，易于拆卸。
采用聚四氟乙烯材料和特殊橡胶化合物密封圈进行密封，可耐受各种溶剂并保持高真空度，使用非常方便。

What is Glass Reactor Trend?

Large volume, this is an effective way and development trend to increase production, reduce quality errors between mass production and reduce product costs.
The stirrer of the glass reactor has been developed from a single stirrer to a forced circulation with a double stirrer or an external pump.
Replace the cumbersome manual operation with production automation and continuity, such as the use of program control, which can not only ensure stable production, improve product quality, increase revenue, reduce manual labor, but also eliminate environmental pollution.

How To Operate Glass Reactors ?

Look:

You should follow these procedures when operating glass reactor:

First, check whether the medium corrodes the main material when you make the reaction of different media in the glass reactor.
When loading the reaction medium, it should not exceed 2/3 of the liquid level of the glass reactor kettle body.
Disassembly under pressure is strictly prohibited! It is strictly forbidden for the kettle to work under the condition of overpressure and overtemperature.
Be careful not to mix water or other liquids when adding heat transfer oil.
Regularly check the swing of the stirring shaft. If the swing is too large, the bearing or sliding sleeve should be replaced in time.
Connect the corresponding voltage according to the usage voltage of the controller.
When the final reaction temperature is determined, it is not allowed to change the temperature setting value during the heating process to avoid a large overshoot of the temperature.

How To Maintain Glass Reactor?

如果您想了解如何维护玻璃反应器，可以参考以下步骤。

用软布擦拭每个接口，然后涂上少许真空吸油膏。
玻璃反应器的接口不应拧得太紧，接头应定期松开，以避免长期卡死导致连接器损坏。
各处的 PTFE 开关都不应拧得过紧，否则容易损坏玻璃。
定期清洁密封圈的方法如下：取下密封圈，检查轴上是否有污垢，用软布擦拭，然后涂上少许真空润滑脂，再重新安装，以保持轴和密封圈之间的光滑。

What is Glass Reactor Precautions

Here are glass reactor precautions :

Before operating the glass reactor, carefully check whether there is any abnormality. During normal operation, do not open the top cover and touch the wiring terminals on the board to avoid electric shock.
The heating speed of the glass reaction kettle should not be too fast, and the pressure should be carried out slowly, especially the stirring speed, only slow rising speed is allowed.
The instrument must not be cooled quickly to prevent damage caused by excessive temperature differential pressure.
When the glass reaction kettle is running, the water jacket between the coupling and the kettle cover must pass cooling water to control the working temperature of the magnetic steel and avoid demagnetization.

Precautions For The Glass Reactor Heat Transfer Oil

When using the heat transfer oil for the first time, there should be no impurities, no mixing of new and old oil, and no chemical liquid dripping into it.

It cannot be heated to a high temperature at one time. It needs to be heated slowly first, and the temperature is slowly raised to allow the oil to be fully heated, so that it can be used for a longer time.

Domestic thermal conductive silicone oil generally boils when it is heated to about 160 degrees.

It is recommended that you choose imported thermal conductive silicone oil, which is colorless, odorless and has a longer service life.

What is Glass Reactor Temperature Control and Decompression Measures?

Glass Reactor Heating Control Measures

For the materials whose reaction temperature is below 90℃, steam and hot water can be used for heating in stages.

First, the temperature should be uniform during heating to avoid local overheating and prevent some materials from deteriorating.

First, use steam to heat to about 60 °C at a medium speed to improve production efficiency, and then use 90 °C hot water to slowly heat up to the specified temperature.

In this way, the staged heating can improve the production efficiency, and at the same time, it can prevent the material from being decomposed by local high temperature or violently vaporized, and can also improve the recovery rate of the material balance reaction and reduce the consumption cost.

Glass Reactor Cooling Control Measures

Look:

The glass reactor cooling system usually used for cooling reaction is mainly jacket cooling and coil cooling.

The cooling liquid used is mainly circulating water and freezing liquid. The cooling rate of the cooling liquid is fast but the cost is high.

During the experiment, if the temperature and pressure rise sharply, you should immediately stay away from the site for personal safety.

Therefore, it is necessary to set an emergency opening of the cooling system button in a slightly far away place, so that the heat source can be quickly cut off for cooling under the premise of ensuring personal safety.

Glass Reactor Explosion Prevention Measures

In order to prevent the material in the three-layer glass reactor from generating a large amount of gas and increasing the pressure when the temperature is out of control, an emergency pressure relief should be set up.

A safety valve should be installed on the top of the glass reactor, if the pressure is too high, the pressure can be released in time.

A bursting disc should be installed for the process that may have a relatively violent reaction, and the outlet of the connecting pipe of the bursting disc must be extended to an outdoor safe place.

Do not point directly to the aisle or operating platform to prevent material splashing and hurting people.

What is Glass Reactor Price?

How much does glass reactor cost?

There shows $2984 for a small glass reactor on internet.

But you should consider the following factors when ask the glass reactor price.

Glass Reactor Design

Here is the deal:

You need to pay more money for a customize design glass reactor than standard type.

Reason?

Cusomized glass reactor requires more design and cost to reach the function.

Standard glass reactor does not need to add extra elements and it does not need more labor to finalize function.

Glass Reactor Volume

Look:

Different volume require different cost and glass reactor manufactuer sell them at different price.

You have to pay more if you choose 20L glass reactor compared to 10L glass reactor.

Glass Reactor Parameter Configuration

Here is the truth:

The more functions, the more configurable parameters, the higher the glass reactor price.

You need to confirm if you need compressive strength, whether there is heating, evaporation, cooling and other functions.

Glass Reactor Brands

Generally, European brands glass reactor price will be higher than China glass reactor.

But you can also find reliable quality glass reactor from China manufacturer.

This is up to your choice.

If you want to use a famous brands glass reactor, you need pay higher price.

But you need to avoid to use vey low price to buy the cheaper glass reactor as it might lead safety issue during your usage.

How To Test the Glass Reactor Tightness?

Look:

Glass reactor can carry out rapid evaporation and fusion reaction.

It can be used in conjunction with various equipment such as low-temperature coolant circulating pump, low-temperature integrated machine, recirculating chillers, refrigerated heating circulator.

Here is the main methods to detect the seal of glass reactor.

Temperature Stress and Confidential Test

The test medium can be used as air, nitrogen, ideally inert gas.

Oxygen or other gases are prohibited.

Temperature Rise Pressure Method

The temperature rise and pressure process must be carried out slowly.

The heating rate does not exceed 80 degrees per hour.

Connect the inlet valve of the compressor or high-pressure pump to the glass reaction part during the pressure test.

Stay for 5 minutes when the working pressure interval rises, and stay for 30 minutes when it rises to the test pressure to observe the sealing condition.

The test pressure should be between 100% and 105%.

When conducting experiments in glass reactor, if air leakage is found, first reduce the pressure, then properly tighten the nuts and joints, and strictly prohibit fixing under high pressure.

How Long Can the Glass Reactor be Kept Under Pressure?

When customers buy glass reactors, they are most worried about the sealing performance of the kettle and whether it can maintain pressure.

The glass reactor needs to be pumped to a negative pressure state to meet the experimental conditions before use.

The pressure range that the glass reactor can withstand: -0.1MPA-0MPA.

The glass reactor will be tested for pressure holding before leaving the factory, and each reactor can be tested for 2 hours under pressure.

After the customer receives the reactor, there will be problems that the pressure is not maintained and the sealing is not enough after the test machine.

At this time, we need to check whether the valve of each glass part is closed and installed.

If necessary, the customer applies vacuum grease to the flange seal. For specific operating procedures, please contact the manufacturer for professional guidance.

What To Do After the Lab Glass Reactor Installation?

Look:

The lab glass reactor cool or heat the reactants at constant temperature through the oil bath.

But what to do after you have installed it?

Here we list the main procedures.

Check for Leaks on Lab Reactor

Check for leaks after a certain amount of nitrogen is introduced to maintain pressure for 30 minutes.

If there is any leakage, please use soap foam to find the leakage point of the pipeline and nozzle. After finding the leakage point, release the gas and tighten it, and then pass the nitrogen pressure test again to ensure that there is no leakage and then start to work normally.

Protection against Excessive Thermal Stress on Lab Glass Reactor

Water can be used for internal cooling through the cooling coil.

Please note that rapid cooling is prohibited to prevent excessive thermal stress from causing cracks on the cooling coil and the kettle body.

At the same time, when the temperature in the kettle exceeds 100 °C, the water jacket between the magnetic stirrer and the kettle cover should be connected with cooling water to ensure that the water temperature is less than 35 °C to avoid demagnetization of the magnetic steel.

The Working Principle of explosion-proof jacketed glass reactor

Here is the truth:

You need to connect with a vacuum device, a high temperature or low temperature circulation device, etc. when putting explosion-proof jacketed glass reactor into use.

You can heat or cool the material during the stir process in the kettle at a constant temperature with hot solution or cooling liquid injected through the interlayer.

When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions.

The solvent vapor is cooled into a liquid when it passes through the glass condensing coil (a cooling device needs to be connected), which can be refluxed into the kettle or recovered through the valve at the lower part of the reflux elbow.

After the reaction is completed, the material can be discharged from the side discharge port at the bottom of the kettle.

What is the pressure resistance of the laboratory glass reactor jacket?

Generally, the pressure of the overall jacket cannot exceed 1MP, otherwise the manufacturing difficulty will be increased due to the large wall thickness of the tank body and the jacket.

When the diameter of the laboratory glass reactor is large or the pressure of the heat transfer medium used is high, the latter three types can be used.

How to Preserve Temperature for Your Glass Reactor

Here is the question:

Will the temperature drop affect the glass reactor?

Look:

If you are in the low temperature area, you should pay special attention to the fact that if the heat transfer medium used in the glass reactor interlayer and condenser tube is water.

You need to pay attention to the freezing condition at low temperature.

In a static state, the water will expand after freezing, which will burst the glass kettle body or the condenser tube.

Therefore, after the experiment, the water in the interlayer and the condenser should be drained to avoid freezing at low temperature.

Most people are facing the problem:

When the temperature drops, it will affect the heating rate of the glass reactor and reduce the efficiency.

Here we list the useful ways to solve this issue.

Use Special Insulation Cotton to Wrap the Glass Reactor

This is the simplest and most direct insulation method. It’s like we wear more clothes when it’s cold. This can effectively prevent excessive temperature loss and provide heating speed.

Properly increase the set temperature of the water-oil bath

Increased bath temperature allows glass reactor to accept higher temperature and shorten heating time.

When the instrument is close to the required operating temperature, lower the temperature of the oil bath to the actual operating temperature.

For example: when the actual operating temperature is 100°C, the temperature of the oil bath can be set to 120°C.

Then when the temperature of the reactor is close to 90 ℃, the temperature of the oil bath can be adjusted to 100 ℃.

This can effectively increase the heating rate and shorten the waiting time.

Do not fill up the solution in the glass reactor at one time

Add solution in batches to increase ramp rate.

The first liquid addition is about half of the capacity, and the temperature is close to the set temperature, and then the material is added to the reaction kettle.

You need to use the above three solutions to keep your glass reactor insulated during use according to your own situation.

The sealing method of glass reactor

Look:

The sealing method of glass reactor include packing sealing and mechanical sealing.

Packing Sealing of Glass Reactor

The packing seal is the gland compresses the packing when the compression bolt is rotated, so that the packing is deformed and adhered to the surface of the shaft to achieve the purpose of sealing.

In chemical production, the shaft seal is easy to leak. Once the toxic gas overflows, it will pollute the environment and even cause an accident. Therefore, it is necessary to control the pressing force.

The elastic deformation of the filler should be large, so that the filler is close to the rotating shaft, and the shrinkage force is generated on the rotating shaft. At the same time, the packing is required to have enough turns.

Mechanical Seal of Glass Reactor

The mechanical seal is composed of four parts: dynamic and static ring, spring loading device and auxiliary seal ring.

Due to the action of the spring force, the dynamic tightness is pressed on the static ring. When the shaft rotates, the spring loading device and the moving ring and other parts rotate together with the shaft, while the static ring is fixed on the seat frame and does not move. The annular sealing end faces that the rings are in contact with prevent material leakage.

Although the structure of the mechanical seal used in the glass reactor is a bit complicated, the sealing effect is very good.

What is The usage instruction of glass reactor

Here is the detail instruction for glass reactor:

Before installation, use, maintenance and inspection, please be sure to read all the contents of the manual carefully and use it correctly.
The power supply voltage must be the same as that specified for this instrument.
No-load operation is not suitable for high-speed operation.
The life of the electrical box is greatly affected by the surrounding temperature and humidity. Please keep the governor and motor dry.
Install the machine first, then wire it by a professional electrician, and turn it on. The ground terminal must be grounded.
Electric shock may still occur due to the discharge of the inverter or capacitor within 5 minutes after the power is turned off.
When working, pay attention to the impact damage to the glass by hard objects.
Be careful when connecting the vacuum pipe and water pipe, so as not to break the glass with excessive force and damage the human body.
When it is necessary to use a high temperature circulating oil bath, pay attention to the damage caused by high temperature to the human body. cleanroom manufacturer china.

What to consider when design glass reactor?

看：

对于玻璃反应器用户来说，安全是最重要的因素。

玻璃反应器制造商在设计玻璃反应器时应考虑安全问题，以确保最终用户的安全。

GWSI 在设计中充分考虑了玻璃反应器的安全性，并将被动温度控制改为主动压力控制。

GWSI玻璃反应器配备排气孔，以达到更高的安全水平。

GWSI 还设计制造了新型防爆双层玻璃反应釜，并配以特殊的防爆电机和与之配套的加热-冷却-制冷循环装置。

在使用过程中应避免气体引起的反应，并尽量保持反应釜环境处于负压或常压状态。

你还应该注意玻璃反应釜表面的温度，不要触摸它，以免烫伤或冻伤。

What are the requirements for the glass reactor reaction material?

Reactants are also considered when designing single and double glass reactors.

The requirements of the reactants in the reactor are as follows.

Compatible or Incompatible Liquids

Mixing of liquids can be easily achieved by constant stirring or mechanical enterprise mixing, and heat transfer of the reaction mixture is carried out by convection data.

Heterogeneous mixing of liquids with solid reactants of appropriate particle size

In this case, it is not possible to mix these materials completely by the mixer. Once the mixing force is gone, the bulk material will settle to the bottom of the kettle, forming a layer of non-conductive material.

The following phenomena occur:

Carbonization of solid reactants, darkening of mixture color, waste of carbonized material, waste of heat and time, non-uniform polymerization, non-uniform polymer composition.

Due to the waste of materials and energy and the impact on the ecological environment, in order to avoid these problems, active materials can be added multiple times in two steps:

First step is to add the liquid reaction material into the reaction kettle, and heat the medium to a temperature slightly higher than the reaction temperature or the melting point of the solid reactant.

Slowly add solid reactants with continuous stirring to allow it to continuously increase the reaction or dissolve to avoid precipitation in the enterprise.

However, it is impossible to maintain this speed, and sometimes the phenomenon of precipitation and coking occurs.

And it takes us a long time to manage in this way to better complete the response.

What is the features for the glass reactor glassware spare part?

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The glass reactor glassware is made of high borosilicate material.

The glass reactor glassware part is heated to a temperature near the glass transition temperature after glass part processing.

Insulation and heating, eliminating the temperature increase and decrease of each part of the glass part.

Relax the stress and remove the stress in the glass parts, so that the appearance of the glass parts is smoother and more beautiful, and the service life is greatly improved.

It can withstand high temperature of 300 degrees Celsius and low temperature of -80 degrees Celsius.

A reliable glass reactor will not fry in high temperature environment and will not break in low temperature environment.

Glass Reactor production must be processed, tested and debugged in strict accordance with the corresponding standards.

According to the different production process and operating conditions, the design structure and parameters of the glass reactor are also different.

How To Solve glass reactor Leakage problem?

Here is the truth:

In the case of improper installation or operation, you will often encounter the situation that the vacuum degree of the glass reactor is not well maintained.

In fact, you don’t need to be nervous and we will provide several ways to solve this problem in the right way.

Here we go.

When installing the glass reactor, the glass joints such as valves and covers should be coated with vacuum grease.
The ceramic bearing (static ring) in the stirring assembly should be tightened, and the inner wall of the assembly should be smeared with vacuum grease.
Mechanical seal ensures full tightening.
Check the looseness of the fasteners daily and tighten them with a wrench.
When the vacuum level of the system is found to be bad, you can use a watering can to spray each glass connection to check for leaks.

How to choose the glass reactor stirring motor?

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The selection of the glass reactor motor is very important.

If you use an inappropriate motor it will directly affect the production progress or damage the glass reactor.

Now we will introduce the tips on how to choose suitable stirring motor for your glass reactor.

Whether the material is viscous

The torque is determined according to the large viscosity of the material.

The reaction is dynamic and the viscosity will also change.

The diameter of the agitator blade and the frontal cross-sectional area, and the speed of the agitation.

Thereby determining the large torque of the motor at this speed to prevent overloading.

The maximum torque of the selected motor should be more than 1.5 of the maximum torque required for the stirring reaction to be safe, and to ensure that the footsteps are always carried out at the required speed.

Choosing a Motor Should Care About Torque, Not Power.

Motors of the same power, at the same speed, the torque is not necessarily the same, especially the AC motor and DC motor, the difference is very large.

As far as a single motor is concerned, the maximum torque is different at different speeds.

Glass Reactor Motor Rotating Speed

This need to decided on your budget.

If the speed requirements are not high, you can choose a geared motor to save your cost if your budget is small.

Is the Glass Reactor Motor Explosion Proof?

If your materials and products are flammable and explosive, an explosion-proof motor should be selected.

And this will cost you more budget compared to the ordianry type motor.

Frequency Control or Manual Adjustment For Glass Reactor Motor

Frequency conversion glass reactor motor will cost more than Manual Adjustment type.

You need to consider which type of motor you need for your glass reactor.

How to care for the glass reactor condenser?

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The condenser is an indispensable part of the glass reactor and plays an important role in quickly converting the vaporized gaseous substances into liquids and quickly transports the heat of the pipes to the air near the pipes.

Since the condensation replaces the cooling tower, the water treatment problem caused by a large amount of water is avoided.

Glass reactor condenser not only greatly reduces the energy conservation and environmental protection but also save your operating cost.

The glass reactor condenser need to be regularly cleaned and maintained in all directions to ensure you have a successful experiement.

Here is the steps on how to maintain the glass reactor condenser.

Check whether the glass reactor works normally, whether there are collision marks, and whether there is a problem with the sealing.
Check and remove the scale condensation affects on glass reactor productivity.

The reason for the Jacketed Glass Reactor explosion

The explosion of the double-layer glass reactor is very dangerous, which threatens people’s life and property in the production test.

It is the top priority to understand the reasons for the explosion of the jacketed glass reactor and effectively curb the occurrence of this phenomenon.

Violent reaction of materials will cause the jacketed glass reactor to burst

Some chemical reactions are exothermic reactions.

When the reaction temperature exceeds the specified temperature, a large amount of gas is generated by the violent reaction of the material, which causes the pressure in the kettle to increase sharply, thereby deforming the inner wall of the double-layer glass fan and causes a large explosion.

Solution:

During the operation, pay attention to control the change of the reaction temperature of the material to prevent the violent reaction caused by the ultra-high temperature.
A pressure relief device is installed to automatically depressurize when the pressure in the kettle increases.

Overpressure of the jacket will cause the jacketed glass reactor to burst

Look:

When chemical enterprises use the steam output by the power plant to supply heat for production, the steam output by the power plant can only be used after decompression.

Once the pressure reducing valve fails, or the safety valve of the steam buffer tank fails, the high-pressure steam output by the power plant is directly input into the double-layer glass reactor jacket.

The overpressure of the jacket is caused, and the wall of the kettle bulges out in a large area due to the external pressure.

Solution:

On the basis of the existing pressure reducing device, a pressure reducing valve is installed, and the first-level pressure reduction is changed to the second-level pressure reduction, so as to achieve double insurance.
The working condition of the pressure reducing valve should be checked frequently, and if any problem is found, it should be replaced immediately.
Check whether the steam safety valve is in correct working condition, especially the spring safety valve should keep it working in a clean environment without corrosion or jamming.

How to control the Glass Reactor temperature of the automatic control system?

The automatic control system of the glass reactor is a commonly used temperature control equipment in the industry.

During the cooling and heating process, the temperature change in the temperature control device is realized through the reciprocating cycle of the medium or refrigerant, so as to achieve the effect of cooling and heating.

Here we list main solutions to control the glass reactor temperature system.

The automatic control system of the reactor has automatic temperature sensing function. The controller adjusts according to the detected temperature and the set temperature value to achieve the purpose of controlling the temperature.
The pressure control generally consists of a high pressure control part and a low pressure control part. When the exhaust pressure exceeds a certain value, the high pressure control of the compressor will cut off the power supply of the compressor, and when the pressure value is lower than a certain value, the low pressure control will also cut off the power supply of the compressor and issue an alarm signal.
In order to prevent the compressor from malfunctioning during high-load operation, the installation of an overheating relay can effectively ensure the overload of the compressor. The lack of phase of a conventional three-phase motor will cause the motor to fail to start or be overloaded. An overload relay can be used to avoid damage to the motor due to lack of phase.
There is a temperature control system at the exhaust port. When the exhaust temperature is too high, the temperature control system will automatically cut off the circuit. Excessive equipment casing temperatures can also affect the compressor. The main reason is that due to the insufficient heat exchange power of the condenser, it is necessary to check its status to see if its air volume, water volume, and water temperature are normal, and check whether there is air entry or other stains in the equipment unit.

Glass Reactor Trouble Shooting Guide

The glassware in the glass reactor is made of double-layer high borosilicate glass and it is popular among many R&D labs.

However, you need to pay attention to the solution of fault problems in the usage process.

Here we list the main technical trouble shooting guide for reference.

The power-on indicator of the glass reactor does not light up

After the power switch is turned on, the indicator light does not light up, you need to find professional electricians to solve the problems of disconnection, looseness, and inability to power on the power supply connected to the equipment, and then debug the equipment after solving the problem.

The glass reactor led is normal, but can’t rotate

The device is powered on and the power is displayed normally, but cannot be rotated.

The rotating shaft is rusted, you can communicate with the supplier in time.

In another case, due to the failure of the motor and power, a professional electrician is called for inspection and repair.

Glass reactor can not complete vacuuming

To check seals for wear, replace seals, maintain vacuum fat regularly.

Vacuum gauge and vacuum pump should also be cleaned regularly.

The vacuum of the glass reactor suddenly disappeared

During use, if the vacuum suddenly disappears during normal use, stop working immediately, confirm whether the glass is cracked, and contact the factory to replace the damaged parts.

How does the glass reactor cool down?

The glass reactor is designed with double-layer glass.

The inner glass layer can be put into the reaction solvent for stirring reaction and the interlayer can be connected to different cold and heat sources for different temperature reaction.

In fact, the cooling and cooling of the glass reactor needs to be strictly operated according to the specified cooling method of the reactor.

This is very important for glass reactor.

If the operation is not follow right cooling way, it will have a bad effect on the glass reactor and you need to pay special attention.

At present, the common cooling methods of glass reactor include water cooling, oil cooling, etc.

Each cooling method has its own advantage.

Therefore, you should use the recommend cooling method required by the manufacturer.

Do not apply the rapid cooling method for your glass reactor.

The glass reactor is a kind of pressure equipment.

It is actually in a special environment when it is working, so quick cooling is prone to lead cracks.

This is particularly bad for the glass reactor.

As the temperature difference stress will greatly damage the reactor from the physics view.

At present, the most common glass reactor cooling method is very simple.

During the cooling process, the user can use water to cool first through the cooling coil so that a better cooling effect can be achieved.

How to Extend the life of laboratory reactor

Here we list practical tips to extend your laboratory glass reactor.

When cleaning the autoclave, special attention should be paid not to let water or other liquids flow into the heating furnace to prevent the heating furnace wire from burning.

If the jacket heat transfer oil is heated, be careful not to add water or other liquids when adding the heat transfer oil, and check the oil level of the heat transfer oil from time to time.

When the reaction temperature is determined, it is not allowed to change the temperature setting value during the heating process, so as to avoid a large overshoot of the temperature.

In order to ensure the normal operation of your lab glass reactor and the personal safety of the staff, please be sure to ground the wire.

When operating, you must pay attention to avoid damage to it due to human reasons, resulting in forced stoppage of production. At the same time, care should be taken to maintain the reactor after use, so as to prolong its service life.

How to feed glass reactor

Look:

The glass reactor is designed with an independent reaction rack.

unlike the industrial reactor with a reaction bench, and the reserved feeding port of glass reactor is small, so the glass reactor feeding process is more difficult.

Here we introduce the practical ways to feed glass reactor.

The feeding amount should not be too large when feeding the glass reactor at one time.

You should evaluate the solvents based on reaction temperature, reflux and pressure for your glass reactor.

You need to add the appropriate amount of ingredients.

Generally, it should not exceed 2/3 of the glass reactor kettle body.

For solid reagents, it is recommended to prepare a solution and add it to the glass reactor.

Liquid reagents can be pumped into the glass reactor through the matching water pump or oil pump.

The reaction material is added to the reaction kettle through a constant pressure dropping funnel or a common dropping funnel, and a corresponding mobile ladder needs to be matched so that the staff can add the test material.